@gus said in Following your documentation – feedback & questions:
I’ve returned to testing the flow cell and even built a second one to check repeatability. I’m wondering what could cause such a large difference in performance between them.
Hey, welcome back! As sepi said, please upload the correct firmware to the MYSTAT as an outdated version was previously present in the repo, also be sure to recalibrate your MYSTAT before cycling again, this is likely the source IMO. It wouldn't be bad to add some sort of calibration reminder/routine into the MYSTAT software...
@sepi said in Following your documentation – feedback & questions:
Good luck with your further investigations! You might want to rzun your future experiments in a transparent PP box in the future. I will for sure once I'm ready for actual electrolyte.
Definitely a good idea!
@gus said in Following your documentation – feedback & questions:
The next day, when I returned to the workshop, both tubes from the pumps had detached from the cell, and the electrolyte had spilled on the table.
Do you have any idea what might have happened?
Ah shoot, sorry to hear this. I suspect if the MYSTAT was out of calibration it may have caused issues with the cycling. An issue with the iodide-containing chemistries is possible clogging of the felts with iodine if something goes wrong; normally the triethylene glycol should prevent this by forming a soluble complex, but it's possible your system got outside the normal operating range. I'd try again fresh (in a PP box/spill tray/secondary containment), with a calibrated MYSTAT running the latest firmware. Tagging @danielfp248 in case he has any suggestions.